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CAS 100-61-8 N-Methylaniline Light Yellow Or Red Brown Oil Liquid

Categories Fuel Oil Additives
Brand Name: JD
Model Number: JD-NMATG-99
Certification: ISO9001
Place of Origin: China
MOQ: 16TONS
Payment Terms: L/C, T/T
Supply Ability: 2000TONS
Delivery Time: 5-8 DAYS
Packaging Details: 200 IRON DRUM
Purity: 90% ,92% ,95%, 99% ,99.5%
Grade: pesticide intermediate, dyestuff intermediate, medicinal intermediate
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CAS 100-61-8 N-Methylaniline Light Yellow Or Red Brown Oil Liquid

N-methylaniline

PHYSICAL PROPERTIES:

Product Name:N-Methylaniline
Synonyms:MONOMETHYLANILINE;N-METHYLANILINE;N-METHYLAMINOBENZENE;N-MONOMETHYLANILINE;(Methylamino)benzene;Benzenamine, N-methyl-;Benzenenamine, N-methyl-;methylaniline(non-specificname)
CAS:100-61-8
MF:C7H9N
MW:107.15
EINECS:202-870-9
Product Categories: Amines;Building Blocks;C7;Chemical Synthesis;Nitrogen Compounds;Organic Building Blocks;Intermediates of Dyes and Pigments;Anilines, Aromatic Amines and Nitro Compounds;Organics;Fine Intermediate;100-61-8
Mol File:100-61-8.mol

N-Methylaniline Chemical Properties
Melting point-57 °C (lit.)
Boiling point196 °C (lit.)
density0.989 g/mL at 25 °C (lit.)
vapor pressure0.5 hPa (20 °C)
refractive indexn20/D 1.571(lit.)
Fp174 °F
storage temp.Store below +30°C.
solubilitywater: slightly soluble30g/L
pka4.84(at 25℃)
formLiquid
colorClear yellow to brown
PH7.6 (1g/l, H2O, 20℃)
OdorModerate aniline-type.
Water Solubility30 g/L
SensitiveAir Sensitive
Merck14,6019
BRN741982
Henry's Law Constant(x 10-5 atm?m3/mol): 1.19 at 25 °C (approximate - calculated from water solubility and vapor pressure)

Specification

ItemIndex
N-methylaniline99%min
Aniline0.2%max
N,N-dimethylaniline0.7%max
Other & moisture0.1%max

PreparationN-methylaniline was synthesized by the reaction of aniline with dimethyl sulfate. Dimethyl sulfate was added dropwise to the mixed solution of aniline and water below 10°C, stirred for 1 h, and then added dropwise with 30% sodium hydroxide solution. The upper layer is the organic phase, and the lower layer is extracted with benzene. After the benzene is recovered from the extract, the obtained oil Chemicalbook-like substance is combined with the organic phase to obtain a mixture of aniline, N-methylaniline and N,N-dimethylaniline. The mixture was treated with sulfuric acid, and the aniline formed sulfate crystals which were filtered off. N,N-dimethylaniline can be converted to N-methylaniline by the following reaction.

APPLICATION:

1. Used as important raw material of pesticide Buprofezin and Mefenacet,
2. Used to make cationic dye .
3.It has wide applications in the field of petroleum additives.(95.0%)


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